Pharmaceutical Drug Analysis

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Pharmaceutical Drug Analysis

GENERAL ASPECTS

Pharmaceutical Chemicals Purity and Management


=> Pharmaceutical Chemicals: Purity and Management
=> Pharmaceutical Chemicals: Purity
=> Pharmaceutical Chemicals: Management
=> Description of the Drug or Finished Product - Pharmaceutical Chemicals: Management
=> Sampling Procedures and Errors - Pharmaceutical Chemicals: Management
=> Bioavailability - Pharmaceutical Chemicals: Management
=> Identification Tests - Pharmaceutical Chemicals: Management
=> Physical Constants - Pharmaceutical Chemicals: Management
=> Limit Tests Vis-A-Vis Quantitative Determinations
=> Various Types of Tests for Quantitative Determinations - Pharmaceutical Chemicals: Management
=> Limit Tests for Metallic Impurities
=> Limit Tests for Lead
=> Limit Test for Arsenic
=> Limit Test’s for Acid Radical Impurities
=> Limit Tests for Non-Metallic Impurities

Theory and Technique of Quantitative Analysis


=> Theory and Technique of Quantitative Analysis
=> Volumetric Analysis
=> Volumetric Apparatus
=> Volumetric Analysis: General Cosiderations
=> Technique of Volumetric Analysis
=> Biomedical Analytical Chemistry
=> Biomedical Analytical Chemistry: Colorimetric Assays
=> Biomedical Analytical Chemistry: Enzymatic Assays
=> Radioimmunoassays (RIAS)
=> Automated Methods of Clinical Analysis

Errors In Pharmaceutical Analysis and Statistical Validation


=> Errors in Pharmaceutical Analysis
=> Classification of Errors in Pharmaceutical Analysis
=> Pharmaceutical Statistical Validation
=> Statistical Treatment of Finite Samples
=> Distribution of Random Numbers
=> Significant Figures
=> Comparison of Results
=> Method of Least Squares
=> Recommendations for Criteria of Rejecting an Observation
=> Sampling Statistics

CHEMICAL METHODS

Aqueous Titrations


=> Aqueous Titrations
=> Theory of Acidimetry
=> Aqueous Titrations: Assay of Drugs
=> Theory of Alkalimetry

Non Aqueous Titrations


=> Non-Aqueous Titrations
=> Non-Aqueous Titrations: Theory
=> Non-Aqueous Titrations: Methodology
=> Assay by Non-Aqueous Titrations
=> Acidimetry in Non-Aqueous Titrations
=> Alkalimetry in Non-Aqueous Titrations

Permanganate Dichromate and Ceric Sulphate Titration Methods


=> Permanganate, Dichromate and Ceric Sulphate Titration Methods
=> Theory - Permanganate, Dichromate and Ceric Sulphate Titration Methods
=> Assay Methods - Permanganate, Dichromate and Ceric Sulphate Titration Methods
=> Permanganate Titration Methods
=> Dichromate Titration Methods
=> Ceric Sulphate Titration Methods

Iodimetric and Iodometric Titrations


=> Iodimetric and Iodometric Titrations
=> Theory - Iodimetric and Iodometric Titrations
=> Assay Methods - Iodimetric and Iodometric Titrations
=> Iodimetric Assays
=> Iodometric Assays
=> Argentometric Precipitation Methods
=> Argentometric Precipitation Methods: Theory
=> Argentometric Precipitation Methods: Assay Methods

Complexometric Analysis


=> Complexometric Analysis
=> Complexometric Analysis: Theory
=> Complexometric Analysis: Assay Methods

Gravimetric Analysis


=> Gravimetric Analysis
=> Gravimetric Analysis: Theory
=> Gravimetric Analysis: Assay Methods
=> Substances Assayed Gravimetrically
=> Substances Assayed After Conversion - Gravimetric Analysis

Thermoanalytical Analysis


=> Thermoanalytical Analysis
=> Thermogravimetric Analysis (TGA)
=> Differential Thermal Analysis (DTA)
=> Thermometric Titrations (TT)

Diazotization Sodium Nitrite Titration


=> Diazotization (Sodium Nitrite Titration)
=> Diazotization (Sodium Nitrite Titration): Assay Methods

Estimation of Phenols and Related Compounds


=> Estimation of Phenols and Related Compounds
=> Estimation of Phenols and Related Compounds: Assay Methods

Karl Fischer Method for Determination of Water


=> Karl Fischer Method for Determination of Water
=> Instrumentation - Karl Fischer Method for Determination of Water
=> Applications of Karl Fischer Method for Determination of Water in Pharmaceutical Analysis

Tetrazolium Assay of Steroids


=> Tetrazolium Assay of Steroids
=> Tetrazolium Assay of Steroids: Theory
=> Assay of Pharmaceutical Substances - Tetrazolium Assay of Steroids

ELECTROCHEMICAL METHODS

Potentiometric Methods


=> Potentiometric Methods
=> Potentiometric Methods: Theory
=> Potentiometric Methods Instrumentation: Electrodes, Automatic Titrator
=> Applications of Potentiometric Titrations in Pharmaceutical Analysis

Amperometric Methods


=> Amperometric Methods
=> Amperometric Methods: Theory
=> Amperometric Methods: Instrumentation
=> Applications of Amperometric Titrations in Pharmaceutical Substances

OPTICAL METHODS

Refractometry


=> Refractometry
=> Refractometry: Theory
=> Refractometry: Instrumentation
=> Determination of Refractive Index of Pharmaceutical Substances
=> Applications of Refractivity

Polarimetry


=> Polarimetry
=> Polarimetry: Theory
=> Polarimetry: Instrumentation
=> Determination of Optical Activity of Pharmaceutical Substances
=> Nephelometry and Turbidimetry
=> Nephelometry and Turbidimetry: Theory
=> Instruments for Nephelometry and Turbidimetry
=> Turbidimetric Assay of Pharmaceutical Substances
=> Nephelometric Assay of Pharmaceutical Substances

Ultraviolet and Absorption Methods


=> Ultraviolet and Absorption Methods
=> Ultraviolet and Absorption Methods: Theory
=> Ultraviolet and Absorption Methods: Instrumentation
=> Ultraviolet and Absorption Methods: Assay Methods

Infrared Spectrophotometry


=> Infrared Spectrophotometry
=> Infrared Spectrophotometry: Theory
=> Infrared Spectrophotometry: Instrumentation
=> Applications of IR-Spectroscopy in Pharmaceutical Assays
=> Applications of IR-Spectroscopy in Analytical Chemistry

Nuclear Magnetic Resonance Spectroscopy


=> Nuclear Magnetic Resonance Spectroscopy
=> Nuclear Magnetic Resonance Spectroscopy: Theory
=> Interpretation of a NMR-Spectrum
=> Nuclear Magnetic Resonance Spectroscopy: Instrumentation
=> Applications of NMR-Spectroscopy in Pharmaceutical Analysis

Emission Spectroscopy


=> Emission Spectroscopy
=> Emission Spectroscopy: Theory
=> Emission Spectroscopy: Instrumentation
=> Applications of Emission Spectroscopy

Flame Spectroscopy


=> Flame Spectroscopy
=> Flame Spectroscopy: Theory
=> Flame Spectroscopy: Instrumentation
=> Applications of Flame Emission Spectroscopy in Pharmaceutical Analysis

Atomic Absorption Spectroscopy


=> Atomic Absorption Spectroscopy
=> Atomic Absorption Spectroscopy: Theory
=> Atomic Absorption Spectroscopy: Instrumentation
=> Important Aspects of Atomic Absorption Spectroscopy
=> Application of Atomic Absorption Spectroscopy in Pharmaceutical Analysis

ASSAY METHODS BASED ON SEPARATION TECHNIEQUES

Liquid Liquid Extraction


=> Liquid-Liquid Extraction
=> Liquid-Liquid Extraction: Theory
=> Factors Influencing Solvent Extraction
=> Emulsion Problem Encountered in Extractions
=> Assay Methods Based on Liquid-Liquid Extraction

Thin Layer Chromatography TLC


=> Thin Layer Chromatography (TLC)
=> Thin Layer Chromatography (TLC): Theory
=> Preparation of Thin Layers on Plates - Thin Layer Chromatography (TLC)
=> Choice of Adsorbents - Thin Layer Chromatography (TLC)
=> Choice Of Solvent System in Thin Layer Chromatography (TLC)
=> Activation of Adsorbent - Thin Layer Chromatography (TLC)
=> Purification of Silica Gel-G Layers - Thin Layer Chromatography (TLC)
=> Spotting of the Components - Thin Layer Chromatography (TLC)
=> Development of Thin Layers - Thin Layer Chromatography (TLC)
=> Special Techniques in Thin Layer Chromatography (TLC)
=> Chemical Reactions on Thin Layer Chromatography (TLC) Plates
=> Combination of Thin Layer Chromatography (TLC) With other Techniques
=> Detection of Components - Thin Layer Chromatography (TLC)
=> Evaluation of the Chromatogram - Thin Layer Chromatography (TLC)
=> Applications of TLC in Pharmaceutical Analysis

Gas Liquid Chromatography GLC


=> Gas Liquid Chromatography (GLC)
=> Gas Liquid Chromatography (GLC): Theory
=> Gas Liquid Chromatography (GLC): Instrumentation
=> Working Techniques for Quantitative Analysis - Gas Liquid Chromatography (GLC)
=> Applications of GLC in Pharmaceutical Analysis
=> High Performance Liquid Chromatography (HPLC)
=> High Performance Liquid Chromatography (HPLC): Theory
=> Instrumentation - High Performance Liquid Chromatography (HPLC)
=> Derivatization - High Performance Liquid Chromatography (HPLC)
=> Applications of High Performance Liquid Chromatography (HPLC) in Pharmaceutical Analysis

Size Exclusion Chromatography


=> Size Exclusion Chromatography
=> Size Exclusion Chromatography: Theory
=> Size Exclusion Chromatography: Apparatus
=> Applications of Size Exclusion Chromatography in Pharmaceutical Analysis

MISCELLANEOUS METHODS

Radioimmunoassay


=> Radioimmunoassay
=> Radioimmunoassay: Theory
=> Radioimmunoassay: Instrumentation
=> Radioimmunoassay: Methodology of the Assay
=> Applications of Radioimmunoassay (RIA) in Pharmaceutical Analysis
=> Novel Applications of Radioimmunoassay(RIA)-Techniques



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